Abstract: The synthesizing conditions of ferrous glycinate chelate using ferrous chloride and glycine as raw materials were studied in this paper.The result showed that the constitution of the product and the recovery of ferrous were considerably affected by p H ,the molar ratio of glycine to ferrous, and the amount of antioxidant.The optimal reaction condition was pH 5.0,the molar ratio of 2:1.The filtrate was treated with organic solvent and the ferrous glycinate chelate was precipitated in ethyl alcohol absolute.Consequently,the chelate can be purified and analyzed by common chemical method. Extraction solvent was also eva luated. The effect of volume ratio of organic solvent to filtrate on the recovery of ferrous was studied. The highest recovery rate of ferrous was obtained at 8:1l of ethyl alcohol absolute to filtrate of ferrous glycinate. The product was characterized by IR and DSC.